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Author:

Cui Yuntao (Cui Yuntao.) | Wang Jinshu (Wang Jinshu.) (Scholars:王金淑) | Liu Wei (Liu Wei.) | Zang Lei (Zang Lei.) | Li Shuo (Li Shuo.) | Li Zhen (Li Zhen.) | Ye Linghan (Ye Linghan.) | Zhou Meiling (Zhou Meiling.)

Indexed by:

EI Scopus SCIE PKU CSCD

Abstract:

The spherical tungsten powder was fabricated by spray-drying method combined with hydrogen reduction using ammonium metatungstate (AMT) as raw materials. The powder morphology, mean particle size, particle size distribution and phase transformation process of reduction were characterized by SEM, TEM, XRD and laser diffraction particle size analyzer, respectively. Results show that the morphology of the powder prepared by spray drying is hollow sphere, and both of AMT and WO3 powder has similar good spherical structure with smooth surface. TEM results indicate that the process parameters, such as the slurry concentration, compressed air flow rate, and liquid feeding rate, play important roles in controlling the performance of AMT microspheres, such as the size distribution. It is found that calcination has no effect on the particle morphology and phase composition. The mean size is increased with the increase of the slurry concentration and compressed air flow rate, but the size distribution changes slightly with different liquid feed rates. The X-ray diffraction patterns indicate that alpha-W phase is obtained after reduction at 550 degrees C for 2 h in hydrogen atmosphere, but WO3 still exists; after reduction at 750 degrees C for 2 h, WO3 disappears, and a-W phase exists in the powder.

Keyword:

spherical tungsten powder cathode materials reduction spray-drying

Author Community:

  • [ 1 ] [Cui Yuntao]Beijing Univ Technol, Coll Mat Sci & Engn, Key Lab New Funct Mat, Minist Educ, Beijing 100124, Peoples R China

Reprint Author's Address:

  • [Cui Yuntao]Beijing Univ Technol, Coll Mat Sci & Engn, Key Lab New Funct Mat, Minist Educ, Beijing 100124, Peoples R China

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Source :

RARE METAL MATERIALS AND ENGINEERING

ISSN: 1002-185X

Year: 2011

Issue: 3

Volume: 40

Page: 507-510

0 . 7 0 0

JCR@2022

ESI Discipline: MATERIALS SCIENCE;

JCR Journal Grade:4

CAS Journal Grade:4

Cited Count:

WoS CC Cited Count: 5

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 9

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