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Author:

Yang, Zhi-Hua (Yang, Zhi-Hua.) | Jia, De-Chang (Jia, De-Chang.) | Zhou, Yu (Zhou, Yu.) | Zhang, Jiu-Xing (Zhang, Jiu-Xing.)

Indexed by:

EI Scopus SCIE

Abstract:

SiB0.5C1.5N0.5 nanopowders were synthesized by mechanical alloying method, and a predominantly amorphous with a small volume fraction of nanocrystalline phase was formed in the powders. The results showed that the crystallites were SiC, and the polytype of SiC were 3C and 6H. SiB0.5C1.5N0.5 powders were consolidated by spark plasma sintering (SPS) technique at 1800 degrees C under different sintering pressure. The grain boundaries of SiC and BCN phase could not be clearly distinguished for the ceramics sintered under 25 MPa. When the pressure increased to 40MPa, SiC phase almost completely crystallized, and its grain size was less than 1 mu m. BCN phase were mainly distributed at boundary of SiC grain. Some amorphous structures were found in the sintered ceramics. Relative densities of the ceramics increased from 76.6% to 92.4%, and mechanical property values increased two or three times with the increase of sintering pressure. For the ceramics sintered under a pressure of 40 MPa, flexural strength, fracture toughness, elastic modulus and Vickers' hardness attained to 311.5 MPa, 3.45 MPa m(1/2), 133.0 GPa and 3.68 GPa, respectively. The mass of the SiBCN ceramics lose by several percent below 930 degrees C in air, and then keep unchanged above 1100 degrees C. (C) 2007 Elsevier B.V. All rights reserved.

Keyword:

mechanical properties microstructure SiB0.5C1.5N0.5 ceramics spark plasma sintering mechanical alloying

Author Community:

  • [ 1 ] [Yang, Zhi-Hua]Harbin Inst Technol, Inst Adv Ceram, Harbin 150080, Peoples R China
  • [ 2 ] [Jia, De-Chang]Harbin Inst Technol, Inst Adv Ceram, Harbin 150080, Peoples R China
  • [ 3 ] [Zhou, Yu]Harbin Inst Technol, Inst Adv Ceram, Harbin 150080, Peoples R China
  • [ 4 ] [Zhang, Jiu-Xing]Beijing Univ Technol, Minist Educ China, Key Lab Adv Funct Mat, Beijing 100022, Peoples R China

Reprint Author's Address:

  • [Yang, Zhi-Hua]Harbin Inst Technol, Inst Adv Ceram, Harbin 150080, Peoples R China

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Source :

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING

ISSN: 0921-5093

Year: 2008

Issue: 1-2

Volume: 488

Page: 241-246

6 . 4 0 0

JCR@2022

ESI Discipline: MATERIALS SCIENCE;

JCR Journal Grade:2

Cited Count:

WoS CC Cited Count: 31

SCOPUS Cited Count: 34

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 8

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