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Author:

Xiao, Yajiao (Xiao, Yajiao.) | Xiong, Xiangyuan (Xiong, Xiangyuan.) | Sun, Guangyan (Sun, Guangyan.) | Sun, Mengju (Sun, Mengju.) | Liu, Wenqing (Liu, Wenqing.)

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EI Scopus SCIE

Abstract:

The 15–5 PH stainless steel was aged at 500 °C for 128 h after solution treatment at 1040 °C for 1 h. The microstructure and composition of each phase in the alloy were characterized by using transmission electron microscopy (TEM) and atom probe tomography (APT). It was found that martensite, retained austenite and reverted austenite contained Cu-rich precipitates and coexisted in the alloy. These precipitates possess face-centered cubic (fcc) structure and orientation relationships with the matrix as following: [113]M//[112]A//[011]Cu and (111¯)Cu//11¯0)M//(111¯)A. But the morphology, size and number density of the precipitates in the three phases are different. In the martensite, the Cu-rich precipitates are coarse, in rod-like shape, up to ~40 nm in length; while in the retained austenite, they are small spherical with an average radius of ~0.8 nm, and coherent with the matrix. In the reverted austenite, the precipitates are large and spheroidal with an average radius of ~2 nm, larger than the size in the martensite but smaller than that in the retained austenite, which could be due to the faster growing of precipitates in martensite than in austenite. © 2022 Elsevier Inc.

Keyword:

High resolution transmission electron microscopy Morphology Probes Austenite Martensite

Author Community:

  • [ 1 ] [Xiao, Yajiao]Institute of Materials, School of Materials Science and Engineering, Shanghai University, Shanghai; 200444, China
  • [ 2 ] [Xiong, Xiangyuan]Faculty of Materials and Manufacturing, Beijing University of Technology, Beijing; 100124, China
  • [ 3 ] [Sun, Guangyan]Institute of Materials, School of Materials Science and Engineering, Shanghai University, Shanghai; 200444, China
  • [ 4 ] [Sun, Mengju]Institute of Materials, School of Materials Science and Engineering, Shanghai University, Shanghai; 200444, China
  • [ 5 ] [Liu, Wenqing]Institute of Materials, School of Materials Science and Engineering, Shanghai University, Shanghai; 200444, China

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Source :

Materials Characterization

ISSN: 1044-5803

Year: 2022

Volume: 191

4 . 7

JCR@2022

4 . 7 0 0

JCR@2022

ESI Discipline: MATERIALS SCIENCE;

ESI HC Threshold:66

JCR Journal Grade:1

CAS Journal Grade:1

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count: 8

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 4

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