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Author:

Wang, Guo-Hong (Wang, Guo-Hong.) | Liu, Xiao-Mei (Liu, Xiao-Mei.) | He, Ding-Yong (He, Ding-Yong.) (Scholars:贺定勇) | Zhou, Zheng (Zhou, Zheng.) (Scholars:周正) | Wang, Zeng-Jie (Wang, Zeng-Jie.) | Wu, Xu (Wu, Xu.)

Indexed by:

EI PKU CSCD

Abstract:

The work aims to study the effects of hydroxyapatite (HA) particle size on the splat morphology and coating microstructure during micro-plasma spraying. Three groups of HA particles with different sizes (25~38 μm, 38~45 μm, 45~63 μm) were selected and the splat particles were collected on the bright finished Ti-6Al-4V substrates and then adopted to deposit HA coatings on sandblasted Ti-6Al-4V substrates by micro-plasma spraying method. The morphologies of splat and coatings were observed by cold field emission scanning electron microscopy (SEM). The phase composition and preferred orientation of the as-sprayed coatings were analyzed through X-ray diffraction (XRD). The three-dimensional morphology characteristics of HA splats were observed by laser scanning confocal microscope (LSCM) and the difference between splats was compared and analyzed. Splats formed during micro-plasma spraying showed distinct morphology characteristics: (i) Oblate spheroid with thicker central area and thinner edge areas; (ii) Disk shaped splats with thinner central area and thicker edge areas, exhibiting a thinner thickness and a larger average diameter compared with oblate shaped splats; and (iii) Disk shaped splats with finger splashing at the rim, having a larger diameter but thickness as same as the disk shaped splats. With the decreasing particle sizes, both the crystallinity and texture intensity of the coatings decreased, while the tendency of HA decomposition and amorphous phase formation increased. Meanwhile, the preferred orientation intensity and the ratio of columnar grains decreased. The morphology of the collected splats and as-sprayed coatings was strongly influenced by the particle sizes during micro-plasma spraying. As the particles sizes increase, the splat morphology was transformed from the oblate spheroid into the disk shape with a small amount of splashing at the rim. The melting degree of the fine powders were better, so the coatings contained more amorphous and decomposed phases with less preference in orientation. © 2019, Chongqing Wujiu Periodicals Press. All rights reserved.

Keyword:

Aluminum alloys Field emission microscopes Crystallinity Aluminum coatings Hydroxyapatite Plasma spraying Textures Titanium alloys Vanadium metallography Scanning electron microscopy Morphology Aluminum metallography Sprayed coatings Ternary alloys Plasma jets Particle size Titanium metallography

Author Community:

  • [ 1 ] [Wang, Guo-Hong]Beijing Engineering Research Center of Eco-materials and LCA, Beijing; 100124, China
  • [ 2 ] [Liu, Xiao-Mei]School of Materials Science and Engineering, Beijing University of Technology, Beijing; 100124, China
  • [ 3 ] [He, Ding-Yong]Beijing Engineering Research Center of Eco-materials and LCA, Beijing; 100124, China
  • [ 4 ] [He, Ding-Yong]School of Materials Science and Engineering, Beijing University of Technology, Beijing; 100124, China
  • [ 5 ] [Zhou, Zheng]Beijing Engineering Research Center of Eco-materials and LCA, Beijing; 100124, China
  • [ 6 ] [Zhou, Zheng]School of Materials Science and Engineering, Beijing University of Technology, Beijing; 100124, China
  • [ 7 ] [Wang, Zeng-Jie]Beijing Engineering Research Center of Eco-materials and LCA, Beijing; 100124, China
  • [ 8 ] [Wu, Xu]Beijing Engineering Research Center of Eco-materials and LCA, Beijing; 100124, China

Reprint Author's Address:

  • 贺定勇

    [he, ding-yong]school of materials science and engineering, beijing university of technology, beijing; 100124, china;;[he, ding-yong]beijing engineering research center of eco-materials and lca, beijing; 100124, china

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Source :

Surface Technology

Year: 2019

Issue: 4

Volume: 48

Page: 91-96

Cited Count:

WoS CC Cited Count: 0

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 8

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