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Author:

Chen, Z. (Chen, Z..) | Duan, W. (Duan, W..) | Zhao, C. (Zhao, C..) | Wang, X. (Wang, X..) | Jin, B. (Jin, B..) | Hu, C. (Hu, C..) | Jia, Q. (Jia, Q..) | Li, S. (Li, S..) | Liu, B. (Liu, B..) | Wang, G. (Wang, G..) | Zhang, D. (Zhang, D..)

Indexed by:

EI Scopus SCIE

Abstract:

Vat photopolymerization 3D printing provides a novel approach for preparing broadband wave-transparent Si3N4/β-SiAlON composite ceramics. This paper oxidized raw powder to introduce low dielectric phases (SiO2) and overcome the low curing depth of α-Si3N4. The solid content of oxidized α-Si3N4 was increased to 50 vol% for the first time by modification with dispersant. The selected print thickness of 50 μm was the highest known for Si3N4 vat photopolymerization 3D printing, greatly improving printing efficiency. Finally, Si3N4/β-SiAlON composite ceramics were sintered in the range of 1600-1800 °C, and the mechanical and dielectric properties were systematically studied. The composite ceramics sintering at 1780 °C had a maximum bending strength of 236 ± 16 MPa, and the real permittivity was 4.83. At 1800 °C the porosity increased resulting in bending strength decreased to 109 ± 4 MPa, and the real permittivity to 3.23. This study filled the gap in the post-treatment of oxidized α-Si3N4 and guided the application of Si3N4/β-SiAlON composite ceramics in the field of wave-transparent. © 2024

Keyword:

Vat photopolymerization 3D printing Powder oxidation Broadband wave-transparent ceramics Si3N4/β-SiAlON composite ceramics

Author Community:

  • [ 1 ] [Chen Z.]Key Laboratory of Space Manufacturing Technology (SMT), Technology and Engineering Centre of Space Utilization, Chinese Academy of Sciences, Beijing, 100094, China
  • [ 2 ] [Chen Z.]Institute for Laser Engineering, School of Physics and Optoelectronic Engineering, Beijing University of Technology, Beijing, 100124, China
  • [ 3 ] [Duan W.]Key Laboratory of Space Manufacturing Technology (SMT), Technology and Engineering Centre of Space Utilization, Chinese Academy of Sciences, Beijing, 100094, China
  • [ 4 ] [Zhao C.]Institute for Laser Engineering, School of Physics and Optoelectronic Engineering, Beijing University of Technology, Beijing, 100124, China
  • [ 5 ] [Wang X.]State Key Lab of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, 430070, China
  • [ 6 ] [Jin B.]School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing, 100083, China
  • [ 7 ] [Hu C.]Key Laboratory of Space Manufacturing Technology (SMT), Technology and Engineering Centre of Space Utilization, Chinese Academy of Sciences, Beijing, 100094, China
  • [ 8 ] [Jia Q.]Key Laboratory of Space Manufacturing Technology (SMT), Technology and Engineering Centre of Space Utilization, Chinese Academy of Sciences, Beijing, 100094, China
  • [ 9 ] [Li S.]Key Laboratory of Space Manufacturing Technology (SMT), Technology and Engineering Centre of Space Utilization, Chinese Academy of Sciences, Beijing, 100094, China
  • [ 10 ] [Liu B.]Key Laboratory of Space Manufacturing Technology (SMT), Technology and Engineering Centre of Space Utilization, Chinese Academy of Sciences, Beijing, 100094, China
  • [ 11 ] [Wang G.]Key Laboratory of Space Manufacturing Technology (SMT), Technology and Engineering Centre of Space Utilization, Chinese Academy of Sciences, Beijing, 100094, China
  • [ 12 ] [Zhang D.]Institute for Laser Engineering, School of Physics and Optoelectronic Engineering, Beijing University of Technology, Beijing, 100124, China

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Source :

Ceramics International

ISSN: 0272-8842

Year: 2024

Issue: 18

Volume: 50

Page: 32549-32560

5 . 2 0 0

JCR@2022

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count: 2

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 5

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