Applications of liquid-phase TEM in the fields of electrocatalysis and photocatalysis - Details

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The　evolution　of　active　sites　at　the　solid-liquid　interface　plays　a　decisive　role　in　determining　the　performance　and　stability　of　electrocatalysis　and　photocatalysis.　As　a　powerful　in　situ　characterization　technique,　Liquid-Phase　Transmission　Electron　Microscopy　(LP-TEM)　offers　unique　opportunities　to　analyze　the　dynamic　reaction　processes　at　solid-liquid　interfaces　with　nano-　or　even　atomic-scale　resolution.　In　this　review,　we　first　trace　the　development　history　of　LP-TEM　technology,　highlighting　its　advantages　for　elucidating　liquid-phase　catalytic　reaction　systems.　Integrating　electrochemical　and　light　illumination　modules　into　LP-TEM　vividly　demonstrates　the　dynamic　evolution　processes　of　electrocatalysis　and　photocatalysis.　Furthermore,　we　systematically　summarize　and　discuss　its　applications　in　the　electrocatalytic　oxygen　evolution　reaction　(OER),　electrocatalytic　CO2　reduction　reaction　(CO2RR),　electrocatalytic　oxygen　reduction　reaction　(ORR),　and　photocatalytic　hydrogen　production,　clarifying　their　current　developmental　status.　Additionally,　we　address　the　limitations　and　challenges　of　the　current　LP-TEM　technique,　such　as　spatial　resolution　and　electron　beam　damage,　providing　insights　for　future　improvements.　©　2025　Elsevier　Ltd

Keyword：

Electrocatalysis Photocatalysis High resolution transmission electron microscopy Nanoclay Oxygen reduction reaction Electrolytic reduction

Author Community：

[ 1 ] [Wang, Yueshuai]Beijing Key Lab of Microstructure and Property of Advanced Materials, College of Materials Science and Engineering, Beijing University of Technology, China
[ 2 ] [Wang, Yueshuai]College of Carbon Neutrality Future Technology, Beijing University of Technology, China
[ 3 ] [Huang, Guoyu]Beijing Key Lab of Microstructure and Property of Advanced Materials, College of Materials Science and Engineering, Beijing University of Technology, China
[ 4 ] [Huang, Guoyu]College of Carbon Neutrality Future Technology, Beijing University of Technology, China
[ 5 ] [Wang, Jiarui]Beijing Key Lab of Microstructure and Property of Advanced Materials, College of Materials Science and Engineering, Beijing University of Technology, China
[ 6 ] [Wang, Jiarui]College of Carbon Neutrality Future Technology, Beijing University of Technology, China
[ 7 ] [Zhao, Hangyi]Beijing Key Lab of Microstructure and Property of Advanced Materials, College of Materials Science and Engineering, Beijing University of Technology, China
[ 8 ] [Zhao, Hangyi]College of Carbon Neutrality Future Technology, Beijing University of Technology, China
[ 9 ] [Li, Zhengli]Beijing Key Lab of Microstructure and Property of Advanced Materials, College of Materials Science and Engineering, Beijing University of Technology, China
[ 10 ] [Li, Zhengli]College of Carbon Neutrality Future Technology, Beijing University of Technology, China
[ 11 ] [Zhang, Zhihong]Beijing Key Laboratory for Magneto-Photoelectrical Composite and Interface Science, State Key Laboratory for Advanced Metals and Materials, University of Science and Technology Beijing, China
[ 12 ] [Sui, Manling]Beijing Key Lab of Microstructure and Property of Advanced Materials, College of Materials Science and Engineering, Beijing University of Technology, China
[ 13 ] [Sui, Manling]College of Carbon Neutrality Future Technology, Beijing University of Technology, China
[ 14 ] [Lu, Yue]Beijing Key Lab of Microstructure and Property of Advanced Materials, College of Materials Science and Engineering, Beijing University of Technology, China
[ 15 ] [Lu, Yue]College of Carbon Neutrality Future Technology, Beijing University of Technology, China

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Source ：

Nano Today

ISSN： 1748-0132

Year： 2025

Volume： 61

1 7 . 4 0 0

JCR@2022

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ESI Highly Cited Papers on the List： 0 Unfold All

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30 Days PV： 6

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