It　is　difficult　to　obtain　a　sharp　cube　texture　through　the　traditional　cold　rolling　and　recrystallization　annealing　procedure　in　the　non-magnetic　and　high　yield　strength　Ni-9.3at%W　(Ni9W)　alloy　due　to　its　low　stacking　fault　energy.　In　this　paper,　a　Ni9W　ingot　with　fine　grain　and　homogenized　tungsten　distribution　was　prepared　by　the　conventional　metallurgy　technique　combined　with　homogenization　annealing　and　intermediate　recrystallization　annealing.　The　rolling　substrate　with　80　mu　m　thickness　was　obtained　through　intensive　cold　rolling　and　four-time　intermediate　recovery　annealing.　The　total　thickness　reduction　was　99%.　A　fraction　of　80.2%　(＜10　degrees)　of　cube　orientation　was　measured　for　the　Ni9W　alloy　tape　through　the　two-step　recrystallization　annealing　method.