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Author:

Liu, W. Q. (Liu, W. Q..) (Scholars:刘卫强) | Yue, M. (Yue, M..) (Scholars:岳明) | Wang, G. P. (Wang, G. P..) | Zhang, D. T. (Zhang, D. T..) (Scholars:张东涛) | Zhang, J. X. (Zhang, J. X..)

Indexed by:

EI Scopus SCIE

Abstract:

An an isotropic Nd-Fe-B magnet was prepared by the spark plasma sintering (SPS) technique. A magnet with the same composition was produced using the conventional sintering method for comparison. The oxidation behavior in oxidizing environments for both magnets was studied. The microstructure and composition of the magnets were investigated using scanning electron microscopy with an energy-dispersive x-ray detector. Compared with the conventional sintered Nd-Fe-B magnet, the SPS magnet possesses a lower oxygen diffusion coefficient, which leads to a lower oxidation rate, a thinner oxidation layer, and lower oxygen Content. Microstructure observation shows that the SPS magnet possesses a unique microstructure due to the special sintering mechanism. In detail, the grain size of the Nd2Fe14B main phase is fine and uniform. Only a little of the Nd-rich phase forms along the grain boundaries of the Nd2Fe14B phase, while most of it agglomerates into triple junctions as small particles. Therefore, the pathways for oxidation propagation are restricted and the intergranular oxidation process through the Nd-rich phase in the magnet is suppressed effectively. As a result, the SPS Nd-Fe-B magnet: possesses better oxidation resistance than that of the conventional magnet.

Keyword:

Nd-Fe-B magnet oxidation resistance microstructure spark plasma sintering

Author Community:

  • [ 1 ] [Liu, W. Q.]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing 100124, Peoples R China
  • [ 2 ] [Yue, M.]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing 100124, Peoples R China
  • [ 3 ] [Zhang, D. T.]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing 100124, Peoples R China
  • [ 4 ] [Zhang, J. X.]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing 100124, Peoples R China
  • [ 5 ] [Wang, G. P.]Jiangxi Normal Univ, Coll Phys & Commun Elect, Nanchang 330022, Peoples R China

Reprint Author's Address:

  • 岳明

    [Yue, M.]Beijing Univ Technol, Coll Mat Sci & Engn, Beijing 100124, Peoples R China

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Source :

CORROSION

ISSN: 0010-9312

Year: 2010

Issue: 5

Volume: 66

1 . 6 0 0

JCR@2022

ESI Discipline: MATERIALS SCIENCE;

JCR Journal Grade:1

CAS Journal Grade:3

Cited Count:

WoS CC Cited Count: 12

SCOPUS Cited Count: 9

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 5

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