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Abstract:
采用放电等离子烧结技术,以氢直流电弧法制备的La-LaH2纳米粉末为原料,制备了高纯LaB6多晶纳米块体热阴极材料.系统研究了LaH2的脱氢反应、SPS合成LaB6的烧结反应式,并用XRD、SEM、TEM和AFM对LaB6烧结块体的相与结构进行了表征.实验结果表明,LaH2在796.4℃时发生脱氢反应;SPS制备得到了单相LaB6纳米多晶块体,纯度达到99.867%,相对密度达到99.2%,和其他烧结方法相比,样品显微硬度及抗弯强度等性能显著提高.晶体为大小均匀,形态规则完整的等轴晶,50MPa,烧结温度1250~1350℃范围内平均晶粒尺寸为120nm,随烧结温度的升高,晶粒尺寸逐渐增大.
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无机材料学报
ISSN: 1000-324X
Year: 2008
Issue: 6
Volume: 23
Page: 1199-1204
1 . 7 0 0
JCR@2022
ESI Discipline: MATERIALS SCIENCE;
JCR Journal Grade:3
Cited Count:
WoS CC Cited Count: 0
SCOPUS Cited Count:
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count: 15
Chinese Cited Count:
30 Days PV: 9
Affiliated Colleges: