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Author:

Yu, Mingchao (Yu, Mingchao.) | Guo, Zhenxi (Guo, Zhenxi.) | Meng, Xin (Meng, Xin.) | Chen, Yongtao (Chen, Yongtao.) | Yu, Jidong (Yu, Jidong.) | Sui, Manling (Sui, Manling.) (Scholars:隋曼龄)

Indexed by:

EI Scopus SCIE

Abstract:

An ??-Fe ??? ??-Fe phase transformation occurs in iron when the shock loading pressure exceeds 13 GPa, but all the ??-Fe will reverse back to ??-Fe during unloading, resulting in no residual ??-Fe in the unloaded samples. To prove the occurrence of this process, a series of microstructural characterization techniques were used to study the microstructures of shock-loaded iron, but hard to reach a consensus on the experimental results. Here, by using two conventional electron microscopy techniques, electron backscattered diffraction (EBSD) in scanning electron microscopy and selected area electron diffraction (SAED) in transmission electron microscopy, we reveal six novel phase transformation variants directly related to the reversible phase transformation. On this basis, the essential differences of microstructure between deformation area and phase transformation area are revealed. Further, we propose two fast and efficient methods which can identify the occurrence of the reversible phase transformation by EBSD and SAED, respectively. The universality of these methods has been verified in different shock loading experiments in iron.

Keyword:

EBSD ?-Fe??-Fe reversible phase transformation Phase transformation variants Deformation twins Shock-loaded iron

Author Community:

  • [ 1 ] [Yu, Mingchao]Beijing Univ Technol, Fac Mat & Mfg, Beijing Key Lab Microstructure & Properties Solid, Beijing 100124, Peoples R China
  • [ 2 ] [Guo, Zhenxi]Beijing Univ Technol, Fac Mat & Mfg, Beijing Key Lab Microstructure & Properties Solid, Beijing 100124, Peoples R China
  • [ 3 ] [Meng, Xin]Beijing Univ Technol, Fac Mat & Mfg, Beijing Key Lab Microstructure & Properties Solid, Beijing 100124, Peoples R China
  • [ 4 ] [Sui, Manling]Beijing Univ Technol, Fac Mat & Mfg, Beijing Key Lab Microstructure & Properties Solid, Beijing 100124, Peoples R China
  • [ 5 ] [Chen, Yongtao]China Acad Engn Phys, Inst Fluid Phys, Mianyang 621900, Peoples R China
  • [ 6 ] [Yu, Jidong]China Acad Engn Phys, Inst Fluid Phys, Mianyang 621900, Peoples R China
  • [ 7 ] [Guo, Zhenxi]Peking Univ, Sch Life Sci, Cryo EM Core Facil, Beijing 100871, Peoples R China

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Source :

MATERIALS CHARACTERIZATION

ISSN: 1044-5803

Year: 2022

Volume: 194

4 . 7

JCR@2022

4 . 7 0 0

JCR@2022

ESI Discipline: MATERIALS SCIENCE;

ESI HC Threshold:66

JCR Journal Grade:1

CAS Journal Grade:1

Cited Count:

WoS CC Cited Count: 2

SCOPUS Cited Count: 2

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 7

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