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Author:

Sun, Honghong (Sun, Honghong.) | Wang, Man (Wang, Man.) | Zhou, Jianing (Zhou, Jianing.) | Xi, Xiaoli (Xi, Xiaoli.) (Scholars:席晓丽) | Nie, Zuoren (Nie, Zuoren.)

Indexed by:

EI Scopus SCIE

Abstract:

The Al-containing particles in ODS alloys with Al addition usually exhibit relatively large size, and inevitably result in a limited improvement in mechanical properties. In this paper, W-Al-Y2O3 alloy was prepared by a two-step sintering process to refine the Al-containing particles. Microstructure evolution of dispersoid particles was characterized by scanning electron microscope (SEM), electron probe microanalysis (EPMA) and transmission electron microscopy (TEM). During the first holding step at 1000 degrees C, the dissolved Al precipitated directly from W matrix, where the formed gamma-Al2O3 particles were nano-sized and developed a coherent relationship with W matrix. This coherent relationship hindered transformation of gamma-Al2O3 into submicron-sized alpha-Al2O3. Moreover, the nano-sized gamma-Al2O3 contributed to formation of fine Y3Al5O12 dispersoid particles with the sintering tem-perature further increased to 1600 degrees C. 71% of the dispersoid particles were distributed within grains and most of them were nano-sized gamma-Al2O3 and Y3Al5O12, giving a fine grain size of 0.49 mu m. Due to the refined micro-structure, the compressive strength and microhardness of W-Al-Y2O3 alloy reached 2545.9 MPa and 787.8 HV, respectively.

Keyword:

Two-step sintering process Al -containing particles Mechanical property Multi -doped W alloy Microstructure

Author Community:

  • [ 1 ] [Sun, Honghong]Beijing Univ Technol, Collaborat Innovat Ctr Capital Resource Recycling, Beijing 100124, Peoples R China
  • [ 2 ] [Wang, Man]Beijing Univ Technol, Collaborat Innovat Ctr Capital Resource Recycling, Beijing 100124, Peoples R China
  • [ 3 ] [Zhou, Jianing]Beijing Univ Technol, Collaborat Innovat Ctr Capital Resource Recycling, Beijing 100124, Peoples R China
  • [ 4 ] [Xi, Xiaoli]Beijing Univ Technol, Collaborat Innovat Ctr Capital Resource Recycling, Beijing 100124, Peoples R China
  • [ 5 ] [Nie, Zuoren]Beijing Univ Technol, Collaborat Innovat Ctr Capital Resource Recycling, Beijing 100124, Peoples R China
  • [ 6 ] [Xi, Xiaoli]Beijing Univ Technol, Natl Engn Lab Ind Big Data Applicat Technol, Beijing 100124, Peoples R China
  • [ 7 ] [Nie, Zuoren]Beijing Univ Technol, Natl Engn Lab Ind Big Data Applicat Technol, Beijing 100124, Peoples R China
  • [ 8 ] [Wang, Man]Beijing Univ Technol, Fac Mat & Mfg, Key Lab Adv Funct Mat, Minist Educ, Beijing 100124, Peoples R China
  • [ 9 ] [Nie, Zuoren]Beijing Univ Technol, Fac Mat & Mfg, Key Lab Adv Funct Mat, Minist Educ, Beijing 100124, Peoples R China
  • [ 10 ] [Xi, Xiaoli]Beijing Univ Technol, Fac Mat & Mfg, 100 Pingleyuan, Beijing 100124, Peoples R China

Reprint Author's Address:

  • [Xi, Xiaoli]Beijing Univ Technol, Fac Mat & Mfg, 100 Pingleyuan, Beijing 100124, Peoples R China;;

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Source :

INTERNATIONAL JOURNAL OF REFRACTORY METALS & HARD MATERIALS

ISSN: 0263-4368

Year: 2023

Volume: 110

3 . 6 0 0

JCR@2022

ESI Discipline: MATERIALS SCIENCE;

ESI HC Threshold:26

Cited Count:

WoS CC Cited Count: 5

SCOPUS Cited Count: 5

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 8

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