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Abstract:
The Al-containing particles in ODS alloys with Al addition usually exhibit relatively large size, and inevitably result in a limited improvement in mechanical properties. In this paper, W-Al-Y2O3 alloy was prepared by a two-step sintering process to refine the Al-containing particles. Microstructure evolution of dispersoid particles was characterized by scanning electron microscope (SEM), electron probe microanalysis (EPMA) and transmission electron microscopy (TEM). During the first holding step at 1000 degrees C, the dissolved Al precipitated directly from W matrix, where the formed gamma-Al2O3 particles were nano-sized and developed a coherent relationship with W matrix. This coherent relationship hindered transformation of gamma-Al2O3 into submicron-sized alpha-Al2O3. Moreover, the nano-sized gamma-Al2O3 contributed to formation of fine Y3Al5O12 dispersoid particles with the sintering tem-perature further increased to 1600 degrees C. 71% of the dispersoid particles were distributed within grains and most of them were nano-sized gamma-Al2O3 and Y3Al5O12, giving a fine grain size of 0.49 mu m. Due to the refined micro-structure, the compressive strength and microhardness of W-Al-Y2O3 alloy reached 2545.9 MPa and 787.8 HV, respectively.
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INTERNATIONAL JOURNAL OF REFRACTORY METALS & HARD MATERIALS
ISSN: 0263-4368
Year: 2023
Volume: 110
3 . 6 0 0
JCR@2022
ESI Discipline: MATERIALS SCIENCE;
ESI HC Threshold:26
Cited Count:
WoS CC Cited Count: 5
SCOPUS Cited Count: 5
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count:
30 Days PV: 8
Affiliated Colleges: