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Author:

Xi, Y. (Xi, Y..) | Xing, J. (Xing, J..) | Jiang, H. (Jiang, H..) | Chen, Y. (Chen, Y..) | Li, J. (Li, J..) | Fan, L. (Fan, L..)

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EI Scopus SCIE

Abstract:

A systematic understanding of the Pore development of high-temperature rocks after different cooling methods can provide a theoretical basis for underground coal gasification, geothermal resource exploitation and other engineering. In this study, thermal-cooling sandstones with three different cooling methods (natural cooling, liquid nitrogen cooling, and water cooling) were tested using nuclear magnetic resonance equipment, and the generation and development of pores and fissures in thermal-treated sandstones were observed. Magnetic resonance imaging was used to analyze the spatial distribution and connectivity of pores in the thermal-treated sandstones. Scanning electron microscopy was used to analyze the thermal damage mechanism of the thermal-cooling sandstone. The results show that the porosity of sandstone increased gradually with the increase of thermal treatment temperature, and the maximum increase of three cooling methods reached 11.52 %, 13.82 % and 17.05 %, and the micropores accounted for the main contribution to the pore development of thermal-cooling treated sandstone. The relationship between sandstone damage and thermal treatment temperature was quantitatively analyzed, and the growth rate of damage coefficients was first slow and then fast, with 500 °C as the change node. Water cooling damage value is the largest, liquid nitrogen cooling damage value is the second, and natural cooling damage value is the smallest. With the gradual increase of thermal treatment temperature, the red area of sandstone magnetic resonance imaging gradually increases and forms a connected area, indicating that the pores of the specimens rapidly expand and penetrate each other to form cracks. The pore development is mainly concentrated in the outside of the specimens due to the cooling rate. The thermal damage mechanism of thermal-cooling sandstone was analyzed. When the sandstone is heated, the mineral particles undergo physical changes (heating expansion and water evaporation) and chemical changes (mineral phase change and ion dissociation), resulting in intergranular and transgranular cracks inside the rock, respectively. On cooling, the mineral grains contract under the influence of thermal stresses, resulting in tensile stress within the rock. Meanwhile, hydrolysis of carbonate mineral and expansion of clay minerals during water cooling further lead to the development of intergranular and transgranular cracks.The superposition effect of the two processes of high temperature and cooling creates huge thermal stresses inside the rock, leading to further development of pores and cracks, and becoming the main reason for the development of thermal damage in sandstone. © 2024 Elsevier Ltd

Keyword:

Sandstone Thermal-cooling Damage mechanism Pore NMR

Author Community:

  • [ 1 ] [Xi Y.]Beijing University of Technology, Beijing, 100124, China
  • [ 2 ] [Xing J.]Beijing University of Technology, Beijing, 100124, China
  • [ 3 ] [Jiang H.]Beijing Information Science and Technology University, Beijing, 102206, China
  • [ 4 ] [Chen Y.]Beijing University of Technology, Beijing, 100124, China
  • [ 5 ] [Li J.]China University of Petroleum-Beijing at Karamay, Karamay, 834000, China
  • [ 6 ] [Li J.]China University of Petroleum-Beijing, Beijing, 102249, China
  • [ 7 ] [Fan L.]Beijing University of Technology, Beijing, 100124, China

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Source :

Construction and Building Materials

ISSN: 0950-0618

Year: 2024

Volume: 440

7 . 4 0 0

JCR@2022

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count: 4

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 1

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