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Abstract：
Symmetrical bisamides of ethylene diamine of type ArCONHCH2CH2NHCOAr undergo anodic C-C bond cleavage in acetonitrile-LiClO4 under controlled-potential electrolysis. The electrogenerated carbocation intermediates react with the solvent acetonitrile to afford unsymmetrical gem-bisamides of type ArCONHCH2NHCOMe in a one-pot reaction. The yields of the latter products are moderate (up to 60%). Other minor products involve two symmetrical gem-bisamides of type ArCONHCH2NHCOAr and MeCONHCH2NHCOMe and fragmentation products (e.g., ArCONHCHO, ArCONH2, and ArCN).
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ORGANIC LETTERS
ISSN： 1523-7060
Year： 2019
Issue： 19
Volume： 21
Page： 7961-7964
5 . 2 0 0
JCR@2022
ESI Discipline： CHEMISTRY;
ESI HC Threshold：166
JCR Journal Grade：1
Cited Count：
WoS CC Cited Count： 12
SCOPUS Cited Count： 11
ESI Highly Cited Papers on the List： 0 Unfold All
WanFang Cited Count：
Chinese Cited Count：
30 Days PV： 7
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