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Author:

Liu, Wenbin (Liu, Wenbin.) | Song, Xiaoyan (Song, Xiaoyan.) (Scholars:宋晓艳) | Zhang, Jiuxing (Zhang, Jiuxing.) | Wang, Kai (Wang, Kai.) | Zhao, Shixian (Zhao, Shixian.) | Wang, Mingsheng (Wang, Mingsheng.) | Liu, Xuemei (Liu, Xuemei.)

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EI Scopus

Abstract:

A novel route for rapid synthesis of ultrafine WC-Co cemented carbides with homogeneous binder phase distribution is reported. The composite powder is produced by in situ reduction-carbonization reactions by using WO2.9, Co3O4 and carbon black as raw powders. The reaction equilibrium and phase stability are studied by thermodynamic calculations. The WC-Co composite powder is condensed by spark plasma sintering (SPS) to obtain the cemented carbides bulk. The sintering temperature is lower than that in the conventional sintering methods by 150C, while the sintering time is remarkably reduced by 3-5 times. The high performances of the hardness and the fracture toughness are obtained. The experimental results confirm that the present processing scheme of in situ reduction-carbonization reactions and subsequent SPS sintering is an efficient way to prepare WC-Co cemented carbides, and is apparently superior to the conventional long-period techniques of preparing composite powder and cemented carbides bulk.

Keyword:

Fracture toughness Cobalt compounds Carbides Extraction Carbon black Spark plasma sintering Powders In situ processing Carbonization Powder metallurgy Carbide tools

Author Community:

  • [ 1 ] [Liu, Wenbin]Key Laboratory of Advanced Functional Materials, Beijing University of Technology, Ministry of Education, Beijing 100022, China
  • [ 2 ] [Song, Xiaoyan]Key Laboratory of Advanced Functional Materials, Beijing University of Technology, Ministry of Education, Beijing 100022, China
  • [ 3 ] [Zhang, Jiuxing]Key Laboratory of Advanced Functional Materials, Beijing University of Technology, Ministry of Education, Beijing 100022, China
  • [ 4 ] [Wang, Kai]Key Laboratory of Advanced Functional Materials, Beijing University of Technology, Ministry of Education, Beijing 100022, China
  • [ 5 ] [Zhao, Shixian]Key Laboratory of Advanced Functional Materials, Beijing University of Technology, Ministry of Education, Beijing 100022, China
  • [ 6 ] [Wang, Mingsheng]Key Laboratory of Advanced Functional Materials, Beijing University of Technology, Ministry of Education, Beijing 100022, China
  • [ 7 ] [Liu, Xuemei]Key Laboratory of Advanced Functional Materials, Beijing University of Technology, Ministry of Education, Beijing 100022, China

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Year: 2008

Page: 393-399

Language: English

Cited Count:

WoS CC Cited Count: 0

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 5

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