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Abstract:
W-based alloys prepared via oxide dispersion strengthening have shown enhanced mechanical performance in previous studies. In this paper, multi-doped W alloys with composition of W-xAl-0.5Y2O3 (x = 0, 0.1, 0.5, 0.9 wt. %) were fabricated via ball milling and spark plasma sintering (SPS), and effects of Al addition on microstructure and mechanical properties were investigated. Types of particles in W-xAl-0.5Y2O3 alloys were identified using the electron probe microanalysis (EPMA) and transmission electron microscopy (TEM), which was closely related with the ratio of Y:Al. Complex Y3Al5O12 particles were observed in all the multi-doped W alloys with addition of Al due to the reaction of 3Y2O3 + 5Al2O3 -> 2Y3Al5O12 at the sintering temperature of 1600 degrees C during SPS process. The atomic ratio of Y:Al in W-0.1Al-0.5Y2O3 was larger than the stoichiometric ratio of Y:Al in Y3Al5O12, leading to remaining Y2O3. However, the ratio of Y:Al was less than the stoichiometric ratio of 3:5 in both W0.5Al-0.5Y2O3 and W-0.9Al-0.5Y2O3, where the particles of Al2O3 were identified consequently. Among these alloys, W-0.5Al-0.5Y2O3 exhibited the most refined microstructure with a uniform distribution of smaller dispersion particles, leading to the superior mechanical strength and ductility.
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MATERIALS CHARACTERIZATION
ISSN: 1044-5803
Year: 2022
Volume: 185
4 . 7
JCR@2022
4 . 7 0 0
JCR@2022
ESI Discipline: MATERIALS SCIENCE;
ESI HC Threshold:66
JCR Journal Grade:1
CAS Journal Grade:1
Cited Count:
WoS CC Cited Count: 11
SCOPUS Cited Count: 11
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count:
30 Days PV: 8
Affiliated Colleges: