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Author:

Yu, L. (Yu, L..) | Lu, Q. (Lu, Q..) | Yang, X. (Yang, X..) | Liu, W. (Liu, W..) | Dong, G. (Dong, G..) | Huang, S. (Huang, S..) | Deng, Y. (Deng, Y..) | Meng, L. (Meng, L..) | Liu, Y. (Liu, Y..) | Yi, X. (Yi, X..) | Yu, J. (Yu, J..) | Wu, Y. (Wu, Y..) | Yue, M. (Yue, M..)

Indexed by:

EI Scopus SCIE

Abstract:

The highly efficient and green recycling of sintered Nd-Fe-B sludge has emerged as a pressing concern in light of the escalating production of sludge. In this work, a novel ultra-short process strategy of purification-remixing incorporation is proposed for in-situ regeneration across several types of Nd-Fe-B sludges. The magnetic properties of the regenerated magnets are effectively restored by remixing the purified sludge at 30 wt% into customized high-remanence magnetic powder, followed by the adjustment of rare earth content to 30.5 % using rare earth-rich compounds. For magnets using 48SH sludge, the remanence and coercivity are recovered to 13.8 kG and 22.2 kOe, respectively, with recovery rates of 97 % and 108.3 %, which are almost as high as those of the original magnets. The temperature stability of the magnet is comparable to that of the original magnet as well. The comprehensive analysis attributes the attainment of high-performance to the repair and optimization of the microstructure, particularly focusing on the grain boundary phase.The ultra-short recovery process and the reuse of solvents in the purification phase minimize the total energy consumption and carbon emissions, and show great potential for green recycling for Nd-Fe-B sludge. © 2024 Elsevier B.V.

Keyword:

Nd-Fe-B sludge In-situ regeneration Ultra-short process Separation and purification

Author Community:

  • [ 1 ] [Yu L.]College of Materials and Engineering, Key Laboratory of Advanced Functional Materials, Ministry of Education of China, Beijing University of Technology, Beijing, 100124, China
  • [ 2 ] [Lu Q.]College of Materials and Engineering, Key Laboratory of Advanced Functional Materials, Ministry of Education of China, Beijing University of Technology, Beijing, 100124, China
  • [ 3 ] [Lu Q.]Earth-Panda Advanced Magnetic Materials Co., Ltd., State Key Laboratory of Rare Earth Permanent Magnetic Materials, Lujiang County, Hefei. Anhui., 231500. PR, China
  • [ 4 ] [Yang X.]College of Materials and Engineering, Key Laboratory of Advanced Functional Materials, Ministry of Education of China, Beijing University of Technology, Beijing, 100124, China
  • [ 5 ] [Liu W.]College of Materials and Engineering, Key Laboratory of Advanced Functional Materials, Ministry of Education of China, Beijing University of Technology, Beijing, 100124, China
  • [ 6 ] [Liu W.]Earth-Panda Advanced Magnetic Materials Co., Ltd., State Key Laboratory of Rare Earth Permanent Magnetic Materials, Lujiang County, Hefei. Anhui., 231500. PR, China
  • [ 7 ] [Dong G.]Baotou Inst Magnetic New Material Co., Ltd., Inner Mongolia, Baotou, 014030, China
  • [ 8 ] [Huang S.]Baotou Inst Magnetic New Material Co., Ltd., Inner Mongolia, Baotou, 014030, China
  • [ 9 ] [Deng Y.]Inner Mongolia Rare Earth Functional Materials Innovation Center Co., Ltd., Inner Mongolia, Baotou, 014030, China
  • [ 10 ] [Meng L.]Inner Mongolia Rare Earth Functional Materials Innovation Center Co., Ltd., Inner Mongolia, Baotou, 014030, China
  • [ 11 ] [Liu Y.]Earth-Panda Advanced Magnetic Materials Co., Ltd., Anhui, Lujiang County, Hefei, 231500, China
  • [ 12 ] [Liu Y.]Earth-Panda Advanced Magnetic Materials Co., Ltd., State Key Laboratory of Rare Earth Permanent Magnetic Materials, Lujiang County, Hefei. Anhui., 231500. PR, China
  • [ 13 ] [Yi X.]Earth-Panda Advanced Magnetic Materials Co., Ltd., Anhui, Lujiang County, Hefei, 231500, China
  • [ 14 ] [Yi X.]Earth-Panda Advanced Magnetic Materials Co., Ltd., State Key Laboratory of Rare Earth Permanent Magnetic Materials, Lujiang County, Hefei. Anhui., 231500. PR, China
  • [ 15 ] [Yu J.]Zhongci Technology Co., Ltd, Wanrong County, Shanxi, Yuncheng, 044000, China
  • [ 16 ] [Wu Y.]College of Materials and Engineering, Key Laboratory of Advanced Functional Materials, Ministry of Education of China, Beijing University of Technology, Beijing, 100124, China
  • [ 17 ] [Yue M.]College of Materials and Engineering, Key Laboratory of Advanced Functional Materials, Ministry of Education of China, Beijing University of Technology, Beijing, 100124, China
  • [ 18 ] [Yue M.]Earth-Panda Advanced Magnetic Materials Co., Ltd., State Key Laboratory of Rare Earth Permanent Magnetic Materials, Lujiang County, Hefei. Anhui., 231500. PR, China

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Source :

Separation and Purification Technology

ISSN: 1383-5866

Year: 2024

Volume: 350

8 . 6 0 0

JCR@2022

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count: 2

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 2

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