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Abstract:
Vat photopolymerization 3D printing provides a novel approach for preparing broadband wave-transparent Si3N4/(3-SiAlON composite ceramics. This paper oxidized raw powder to introduce low dielectric phases (SiO2) and overcome the low curing depth of alpha-Si3N4. The solid content of oxidized alpha-Si3N4 was increased to 50 vol% for the first time by modification with dispersant. The selected print thickness of 50 mu m was the highest known for Si3N4 vat photopolymerization 3D printing, greatly improving printing efficiency. Finally, Si3N4/(3-SiAlON composite ceramics were sintered in the range of 1600-1800 degrees C, and the mechanical and dielectric properties were systematically studied. The composite ceramics sintering at 1780 degrees C had a maximum bending strength of 236 +/- 16 MPa, and the real permittivity was 4.83. At 1800 degrees C the porosity increased resulting in bending strength decreased to 109 +/- 4 MPa, and the real permittivity to 3.23. This study filled the gap in the posttreatment of oxidized alpha-Si3N4 and guided the application of Si3N4/(3-SiAlON composite ceramics in the field of wave-transparent.
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CERAMICS INTERNATIONAL
ISSN: 0272-8842
Year: 2024
Issue: 18
Volume: 50
Page: 32549-32560
5 . 2 0 0
JCR@2022
Cited Count:
WoS CC Cited Count: 3
SCOPUS Cited Count: 3
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count:
30 Days PV: 4
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