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Author:

Xiao, Y. (Xiao, Y..) | Zhang, L. (Zhang, L..) | Liu, T. (Liu, T..) | Sun, Q. (Sun, Q..) | Song, X. (Song, X..) | Fang, Y. (Fang, Y..) | Li, A. (Li, A..) | Zhu, M. (Zhu, M..) | Li, W. (Li, W..)

Indexed by:

EI Scopus SCIE

Abstract:

The microstructure of (Nd, Ce)–Fe–B sintered magnets with different diffusion depths was characterized by a magnetic force microscope, and the relationship between the magnetic properties and the local structure of grain boundary diffused magnets is discussed. The domains perpendicular to the c-axis (easy magnetization direction) show a typical maze-like pattern, while those parallel to the c-axis show the characteristics of plate domains. The significant gradient change is shown in the concentration of Dy with the direction of diffusion from the surface to the interior. Dy diffuses along grain boundaries and (Dy, Nd)2Fe14B layer with a high anisotropy field formed around the grains. Through in-situ electron probe micro-analysis/magnetic force microscopy (EPMA/MFM), it is found that the average domain width decreases, and the proportion of single domain grains increases as diffusion depth increases. This is caused by both the change of concentration and distribution of Dy. The grain boundary diffusion process changes the microstructure and microchemistry inside the magnet, and these local magnetism differences can be reflected by the configuration of the magnetic domain structure. © 2024 Chinese Society of Rare Earths

Keyword:

Magnetic microstructures Rare earths Magnetic force microscope Grain boundary diffusion process (GBDP) In-situ Ce)–Fe–B (Nd

Author Community:

  • [ 1 ] [Xiao Y.]Division of Functional Materials, Central Iron and Steel Research Institute, Beijing, 100081, China
  • [ 2 ] [Zhang L.]Key Laboratory of Advanced Functional Materials, Ministry of Education of China, College of Materials Science and Engineering, Beijing University of Technology, Beijing, 100124, China
  • [ 3 ] [Liu T.]Division of Functional Materials, Central Iron and Steel Research Institute, Beijing, 100081, China
  • [ 4 ] [Sun Q.]Division of Functional Materials, Central Iron and Steel Research Institute, Beijing, 100081, China
  • [ 5 ] [Song X.]Division of Functional Materials, Central Iron and Steel Research Institute, Beijing, 100081, China
  • [ 6 ] [Fang Y.]Division of Functional Materials, Central Iron and Steel Research Institute, Beijing, 100081, China
  • [ 7 ] [Li A.]Division of Functional Materials, Central Iron and Steel Research Institute, Beijing, 100081, China
  • [ 8 ] [Zhu M.]Division of Functional Materials, Central Iron and Steel Research Institute, Beijing, 100081, China
  • [ 9 ] [Li W.]Division of Functional Materials, Central Iron and Steel Research Institute, Beijing, 100081, China

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Source :

Journal of Rare Earths

ISSN: 1002-0721

Year: 2025

Issue: 3

Volume: 43

Page: 556-568

4 . 9 0 0

JCR@2022

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 9

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