In　order　to　improve　the　homogeneity　of　spherical　Fe-rich　particles　within　the　Cu-rich　matrix,　the　Cu95Fe5　(wt%)　immiscible　composite　coating　has　been　produced　by　the　combination　of　mechanical　alloying　and　laser　cladding.　The　results　show　that　the　milled　composite　powder　presents　a　polygonal　morphology　and　is　mainly　composed　of　face-centered-cubic　(fcc)-Cu　solid　solution.　The　demixing　or　delimitation　is　eliminated　in　the　immiscible　composite　coating　produced　by　laser　cladding　and　large　amounts　of　spherical　alpha-Fe　particles　are　dispersed　within　the　epsilon-Cu　matrix　as　a　result　of　liquid　phase　separation　(LPS).　The　size　of　the　Fe-rich　particles　measured　is　in　radius　of　similar　to　1.5　mu　m,　which　is　much　smaller　than　the　calculated　critical　radius　(similar　to　2.3　mu　m),　confirming　that　the　alpha-Fe　particles　containing　a　supersaturated　Cu　are　driven　by　the　dominant　mechanism　of　Marangoni　motion.　Compared　to　Brass,　the　immiscible　composite　coating　exhibits　the　improved　homogeneous　microhardness　(153HV(0.2))　and　higher　corrosion　resistance,　as　well　as　a　saturated　magnetization　of　similar　to　9.19　emu/g　and　low　coercivity　of　similar　to　9.25　Oe.　(C)　2018　Elsevier　B.V.　All　rights　reserved.