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Author:

Zhang Gaimei (Zhang Gaimei.) | He Cunfu (He Cunfu.) (Scholars:何存富) | Wu Bin (Wu Bin.) (Scholars:吴斌) | Chen Qiang (Chen Qiang.)

Indexed by:

EI Scopus SCIE CSCD

Abstract:

Traditional technique such nanoindenter(NI) can't measure the local elastic modulus at nano-scale(lateral). Atomic force acoustic microscopy (AFAM) is a dynamic method, which can quantitatively determine indentation modulus by measuring the contact resonance spectra for high order modes of the cantilever. But there are few reports on the effect of experimental factors, such length of cantilever, contact stiffness on measured value. For three different samples, including copper(Cu) film with 110 nm thickness, zinc(Zn) film of 90 nm thickness and glass slides, are prepared and tested, using referencing approach in which measurements are performed on the test and reference samples (it's elastic modulus is known), and their contact resonance spectra are measured used the AFAM system experimentally. According to the vibration theory, from the lowest two contact resonance frequencies, the tip-sample contact stiffness is calculated, and then the values for the elastic properties of test sample, such as the indentation modulus, are determined. Using AFAM system, the measured indentation modulus of copper nano-film, zinc nano-film and glass slides are 113.53 GPa, 87.92 GPa and 57.04 GPa, which are agreement with literature values M (Cu) = 105-130 GPa, M (Zn) = 88.44 GPa and M (Glass) = 50-90 GPa. Furthermore, the sensitivity of contact resonance frequency to contact stiffness is analyzed theoretically. The results show that for the cantilevers with the length 160 mu m, 225 mu m and 520 mu m respectively, when contact stiffness increases from 400 N/m to 600 N/m, the increments of first contact resonance frequency are 126 kHz, 93 kHz and 0.6 kHz, which show that the sensitivity of the contact resonance frequency to the contact stiffness reduces with the length of cantilever increasing. The novel method presented can characterize elastic modulus of near surface for nano-film and bulk material, and local elasticity of near surface can be evaluated by optimizing the experimental parameters using the AFAM system.

Keyword:

atomic force acoustic microscope(AFAM) referencing approach contact stiffness local elasticity

Author Community:

  • [ 1 ] [Zhang Gaimei]Beijing Univ Technol, Coll Mech Engn & Appl Elect Technol, Beijing 100124, Peoples R China
  • [ 2 ] [He Cunfu]Beijing Univ Technol, Coll Mech Engn & Appl Elect Technol, Beijing 100124, Peoples R China
  • [ 3 ] [Wu Bin]Beijing Univ Technol, Coll Mech Engn & Appl Elect Technol, Beijing 100124, Peoples R China
  • [ 4 ] [Zhang Gaimei]Beijing Inst Graph Commun, Lab Plasma Phys & Mat, Beijing 102600, Peoples R China
  • [ 5 ] [Chen Qiang]Beijing Inst Graph Commun, Lab Plasma Phys & Mat, Beijing 102600, Peoples R China

Reprint Author's Address:

  • 何存富

    [He Cunfu]Beijing Univ Technol, Coll Mech Engn & Appl Elect Technol, Beijing 100124, Peoples R China

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Source :

CHINESE JOURNAL OF MECHANICAL ENGINEERING

ISSN: 1000-9345

Year: 2012

Issue: 6

Volume: 25

Page: 1281-1286

4 . 2 0 0

JCR@2022

ESI Discipline: ENGINEERING;

JCR Journal Grade:4

CAS Journal Grade:4

Cited Count:

WoS CC Cited Count: 2

SCOPUS Cited Count: 3

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 15

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