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Abstract:
Uniform scandium doped tungsten powder was prepared by sol-gel method combined with reduction process, and then the scandium doped impregnated cathode was successfully prepared by microwave sintering. The characteristics of Sc-doped tungsten powder, the microstructure of cathode sponge matrix, the emission properties, and the surface behavior of the active substance were analyzed. The result shows that the scandium doped tungsten powder has the average size of around 1 µm and Sc element is uniformly distributed. The morphology of the sponge skeleton is spherical, the pore distribution is uniform, the average pore diameter is about 0.46 μm, and scandium is evenly distributed in the matrix. The cathode prepared by the microwave sintering method exhibits good emission properties, e.g., the current density of this cathode reaches 137.59 A/cm2 at 950℃b, and the emission slope is 1.431. The atomic ratio of Ba:Sc:O on the cathode surface is 1.8:1:2.2 after activation, and a large amount of nanoparticles are present on the cathode surface, which promotes emission of the cathode. © 2020, Science Press. All right reserved.
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Rare Metal Materials and Engineering
ISSN: 1002-185X
Year: 2020
Issue: 5
Volume: 49
Page: 1766-1772
0 . 7 0 0
JCR@2022
ESI Discipline: MATERIALS SCIENCE;
ESI HC Threshold:169
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ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
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30 Days PV: 6
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