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Author:

Wang, R. (Wang, R..) | Li, S. (Li, S..) | Hu, P. (Hu, P..) | Chen, S. (Chen, S..) | Wang, J. (Wang, J..)

Indexed by:

Scopus

Abstract:

Fabrication of full-densified Mo metal with fine grain size and uniform microstructure is highly desired to improve its mechanical property. In this work, microwave-field-assisted thermal sintering was utilized to promote the fast densification of Mo nanocrystals, and the compact with high relative density of 99.8 % and fine grain size of 2.09 μm was obtained at 1450°C for 0.5 h with heating rate of 20°C/min, which is much superior to the compact with density of 99.13 % and grain size of 7 μm fabricated by traditional thermal sintering at 1500°C for 1 h. Further theoretical and experimental investigation reveals that effective volume heating transfer with low activation energy provides strong driven-force for densification of nanosized Mo powder at low temperature.  © Engineered Science Publisher LLC 2021.

Keyword:

Nanocrystalline molybdenum Microwave sintering Kinetics Densification Multiphysics simulation

Author Community:

  • [ 1 ] [Wang R.]Key Laboratory of Advanced Functional Materials, Education Ministry of China, Faculty of Materials and Manufacture, Beijing University of Technology, Beijing, 100124, China
  • [ 2 ] [Wang R.]School of Metallurgical Engineering, Xi'an University of Architecture and Technology, Shaanxi, 710043, China
  • [ 3 ] [Li S.]Key Laboratory of Advanced Functional Materials, Education Ministry of China, Faculty of Materials and Manufacture, Beijing University of Technology, Beijing, 100124, China
  • [ 4 ] [Hu P.]Key Laboratory of Advanced Functional Materials, Education Ministry of China, Faculty of Materials and Manufacture, Beijing University of Technology, Beijing, 100124, China
  • [ 5 ] [Chen S.]Key Laboratory of Advanced Functional Materials, Education Ministry of China, Faculty of Materials and Manufacture, Beijing University of Technology, Beijing, 100124, China
  • [ 6 ] [Wang J.]Key Laboratory of Advanced Functional Materials, Education Ministry of China, Faculty of Materials and Manufacture, Beijing University of Technology, Beijing, 100124, China

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Source :

ES Materials and Manufacturing

ISSN: 2578-0611

Year: 2021

Volume: 13

Page: 97-105

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count: 22

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 9

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