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Abstract:
To obtain high-surface-area porous γ-Al2O3, the alco-hydrothermal method was adopted to synthesize plate-shaped wormhole-like mesoporous γ-Al2O3 particles with a face-centered cubic crystal structure, and characterized the physical properties of these materials by means of the X-ray diffraction, N2 adsorption-desorption, scanning electron microscopy, transmission electron microscopy, and selected area electron diffraction techniques. It has been shown that mesoporous γ-Al2O3 particles with the wormhole-like morphology and good crystalinity can be fabricated with aluminum tri-sec-butoxide as the aluminum source, 1-propanol aqueous solution as the solvent, and lauric acid as the template (the mass ratio of aluminum tri-sec-butoxide to lauric acid = 4:1). The surface area of the Al2O3 sample obtained at 600C calcination was up to 306 m2/g and its average pore diameter was ca. 5 nm.
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Journal of Beijing University of Technology
ISSN: 0254-0037
Year: 2008
Issue: 7
Volume: 34
Page: 750-754
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ESI Highly Cited Papers on the List: 0 Unfold All
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30 Days PV: 6
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