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Author:

Zhang, Lei (Zhang, Lei.) | Dai, Hong-Xing (Dai, Hong-Xing.) (Scholars:戴洪兴) | Lu, Xin-Yue (Lu, Xin-Yue.) | Wang, Guo-Zhi (Wang, Guo-Zhi.) | He, Hong (He, Hong.) (Scholars:何洪)

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EI Scopus PKU CSCD

Abstract:

To obtain high-surface-area porous γ-Al2O3, the alco-hydrothermal method was adopted to synthesize plate-shaped wormhole-like mesoporous γ-Al2O3 particles with a face-centered cubic crystal structure, and characterized the physical properties of these materials by means of the X-ray diffraction, N2 adsorption-desorption, scanning electron microscopy, transmission electron microscopy, and selected area electron diffraction techniques. It has been shown that mesoporous γ-Al2O3 particles with the wormhole-like morphology and good crystalinity can be fabricated with aluminum tri-sec-butoxide as the aluminum source, 1-propanol aqueous solution as the solvent, and lauric acid as the template (the mass ratio of aluminum tri-sec-butoxide to lauric acid = 4:1). The surface area of the Al2O3 sample obtained at 600C calcination was up to 306 m2/g and its average pore diameter was ca. 5 nm.

Keyword:

Morphology Surface active agents Hydrothermal synthesis Mesoporous materials Electron diffraction Aluminum oxide Gamma rays Trichloroethylene Crystal structure High resolution transmission electron microscopy Scanning electron microscopy Activated alumina Saturated fatty acids

Author Community:

  • [ 1 ] [Zhang, Lei]Laboratory of Catalysis Chemistry and Nanoscience, College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100022, China
  • [ 2 ] [Dai, Hong-Xing]Laboratory of Catalysis Chemistry and Nanoscience, College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100022, China
  • [ 3 ] [Lu, Xin-Yue]Laboratory of Catalysis Chemistry and Nanoscience, College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100022, China
  • [ 4 ] [Wang, Guo-Zhi]Laboratory of Catalysis Chemistry and Nanoscience, College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100022, China
  • [ 5 ] [He, Hong]Laboratory of Catalysis Chemistry and Nanoscience, College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100022, China

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Source :

Journal of Beijing University of Technology

ISSN: 0254-0037

Year: 2008

Issue: 7

Volume: 34

Page: 750-754

Cited Count:

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ESI Highly Cited Papers on the List: 0 Unfold All

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Chinese Cited Count:

30 Days PV: 6

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